Platinum purification at Impala’s EPMR


Mineral-wool reinforced insulation and piping under the bromate hydrolysis glass-lined vessels.
 

impalapld.jpg (5927 bytes)
Platinum salt separation section with the separation centrifuge in the left foreground and standby glove-box filter to the right.
 

 
The new platinum purifcation section at Impala Platinum Limited-Refneries, Springs, is an addition to the enhanced precious metals refinery (EPMR) completed by BATEMAN in 1997.A classical platinum refining route is used in the new plant, with two signifcant new pieces of equipment added to improve the process. The first is an automated Nutsche pressure filter for the removal of insoluble impurities, and the second is a Peeler centrifuge for the separation of the pure platinum salt.
 

Bromate hydrolysis glass-lined vessels with mineral-wool reinforced insulation and polyvinylidene fuoride (PVDF) pipework.
 

The bromate mud filtration system with Nutsche pressure filter.

Hot commissioning of the plant was accomplished in a minimum of time, and within two weeks of operations commencing, all the mainline platinum was routed through the platinum purifcation section. The product meets Impala’s stringent purity specifcations. The project was completed in accordance with operational requirements and within the budgeted cost. This project was the latest of a sequence of projects undertaken at Springs by BATEMAN for Impala Platinum Limited-Refineries.


Platinum salt precipitation glass-lined vessels, glass condensers and polypropylene pipework.

Integrated project team
A feature of this EPCM project was the way in which an integrated team of personnel from both Impala and BATEMAN tackled the project. The bulk of the work was in fact done out of Impala’s Springs offices, greatly facilitating team-working relationships during the project and the hand over of the facility to the client on its conclusion.

Impala supplied all of the basic design criteria while BATEMAN brought its decades of project experience on the processing of platinum group metals (PGMs) to the team. BATEMAN also led the hazard and operability studies (Hazops), which ensured that the commissioning of the new equipment proceeded smoothly. Besides the normal operational requirements of the plant, the project team also ensured that Impala’s specifcations in respect of security, health and safety were met.

Platinum processing
Platinum refining involves allergenic metal salts and dangerous and corrosive chemicals. This means that exotic materials are needed, such as titanium, glass reinforced plastics (GRP), glass (used for pipelines, condensers, ion exchange columns and the lining of reaction vessels), SAF 2205 stainless steel, carbon-block heat exchangers, polypropylene and polyvinylidene fuoride piping and tanks. The plant design and methods of construction require specialist experience and are often onerous. All emissions from the plant are channelled through a bag filter to eliminate the release of platinum salts to the atmosphere.

Safety
In respect of safety, the project team maintained BATEMAN’s good record, with no disabling injuries occurring during the 156 760 man-hours worked on the project.


Platinum salt bag filter unit extracting air from the separation centrifuge.

Project statistics

Client: Impala Platinum Limited-Refneries
Location: Springs, RSA
Contract: Type EPCM Duration
Planning November 1997
Budget estimate March 1998
First platinum produced June 1999
Plant hand over August 1999
Total project man-hours 156 760 hours
Peak labour force 100
Disabling injuries Nil