Angouran zinc demonstration plant

A demonstration plant, designed, constructed and operated by BATEMAN for the Iran Zinc Mines Development Corporation (IZMDC), confirmed the process route selected for the feasibility study on a proposed refinery for the Angouran Mine, which could produce 100 000 t/yr of zinc from an ore feed of 473 000 t/yr. The plant was located at IZMDC's research centre, about 20 km from Zanjan in north west Iran.

The tests provided an insight into the distribution and accumulation of elemental impurities during the various process stages, essential for optimised plant design and enhanced process control, and to determine the capital cost of the full scale plant. During the five-week test, nearly 20 t of 12 different blends of ore were processed to produce more than 2 t of zinc cathode assaying between 99,99 and 99,995 % purity.

This achievement confirmed BATEMAN's extensive experience in the refining of zinc that the attainment of super-high grade (SHG) zinc cathode is contingent on the use of high-quality reagents and avoiding the contamination of the electrowinning (EW) solutions. Careful management of the entire reagent supply chain proved to be vital.

The Angouran ore consists mainly of carbonates of zinc, lead and calcium, some troublesome minor elements such as arsenic and cadmium and quartz, mica and other silicates. It is considered to be high grade, averaging 23 % zinc.

The demonstration plant comprised circuits for repulping the ore, acid, weak-acid and neutral leaching, residue filtration, copper, cadmium, cobalt and nickel removal, basic-zinc-sulphate precipitation, tailings neutralisation, solvent extraction (SX), EW and reagent mixing and distribution.

The demonstration plant was constructed by modifying an existing hydrometallurgical plant, producing about 120 t/yr of zinc cathode. Modifications included installing new leaching, SX, EW, tailings-neutralisation and electrolyte-cooling circuits. The SX circuit used DEHPA diluted with kerosene as the organic phase and featured Bateman Reverse-Flow Mixer Settlers incorporating extraction, stripping, scrubbing and organic regeneration. Bateman Pulsed Columns were also used to test the SX unit operations.

As protection against inclement weather, which during winter features sub-zero temperatures, the plant was housed in a roofed building with an area of about 1 600 m². A boiler room, metallurgical and analytical laboratories, equipment and electrolyte storage, water treatment facilities, power supplies and motor control centre were also provided.

An Iranian contractor in partnership with BATEMAN's engineering-design team took three months to complete the modifications and commissioning took seven weeks. Local personnel, including masters-degree students, were trained during the commissioning and ramp-up phases and were retained as operating staff during the test campaign. Assays were performed in the on-site laboratories by recruiting temporary personnel from IZMDC and Iranian academic institutions.

More information may be obtained from

Tony Cau, General Manager, Copper, Zinc & Light Metals on
+61-7-3320-333 or email basemetals@batemanengineering.com; or

Richard Klue, BATEMAN Business Manager, Lead & Zinc, on +27-11-899-2651 or email basemetals@batemanengineering.com.

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